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LONGFENG LI1, XIAOWEN LUAN1, CHEN FENG1, JIAN JIANG1, QINGYA YANG1, MINMIN CHEN1, MAOLIN ZHANG1,*
Nano Cu2O/Ca(OH)2 composites are successfully synthesized by a facile, one pot and interface reduction method. The synthesis of these nano composites is accomplished through the reaction of CuCl2 with Ca(OH)2 on its interfac e forming Cu(OH)2/Ca( 2 composite precursor, followed by a reduction of Cu(OH) 2 to Cu2O with glucose as the reducing agent. The as synthesized samples have been characterized by X ray diffraction. The results show that the as synthesized samples are cubi c nanocrystalline Cu2O/Ca(OH)2 composites with Cu2O average crystallite size distribution within a narrow range, indicating that the Ca(OH)2 as a carrier has a controlling effect on the Cu2O average crystallite size. In addition, the average crystallite si ze of Cu2O in Cu2O/Ca(OH) 2 composites was controlled by reaction temperature or the starting concentration of CuCl2. But, reaction time has less impact on crystallinity and size of Cu2O in Cu2O/Ca(OH)2 composites..
Nanocomposites, Cu2O/ Ca(OH)2, Interface reduction method, Synthesis.
LONGFENG LI, XIAOWEN LUAN, CHEN FENG, JIAN JIANG, QINGYA YANG, MINMIN CHEN, MAOLIN ZHANG, A facile one-pot green synthesis of nano-C u 2 O C a( OH 2 composite by an interface reduction method, Optoelectronics and Advanced Materials - Rapid Communications, 8, 9-10, September-October 2014, pp.876-879 (2014).
Submitted at: Feb. 7, 2014
Accepted at: Sept. 11, 2014
Optoelectronics and Advanced Materials - Rapid Communications
(2023): 0.5 - 2023 Journal Citation Reports (Clarivate Analytics, 2024)
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