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Effect of alumina addition on the microstructure properties of plasma-sprayed zirconia-alumina coatings

SERKAN ISLAK1,*

Affiliation

  1. Kastamonu University, Faculty of Engineering and Architecture, Department of Materials Science and Nanotechnology Engineering, 37000, Kastamonu, Turkey

Abstract

ZrO2/Al2O3 coatings with different amounts of Al2O3 were fabricated on the AISI 304 stainless steel surface using plasma spray process. Phase composition and microstructure of the coatings were characterised using X-ray diffraction and scanning electron microscopy. Lamellae and porous microstructure were obtained in the coatings. In addition, a small amount of unmelted particles, partially melted, and fully melted regions in microstructure of coatings were observed. With the increasing addition of Al2O3, a decrease in the pores was determined. The results indicated that the as-prepared ZrO2/Al2O3 based coatings were mainly composed of ZrO2, Al0.52Zr0.48O1.74, ZrTiO4, Al0.18Zr0.82O1.91, Al2O3, Al2Zr3, Al3Ti and Ti2O3 phases. The microhardness of the coating was as high as 1136 HV0.2, which was 4-5 times of the substrate..

Keywords

Plasma spray, ZrO2, Al2O3, Microstructure.

Citation

SERKAN ISLAK, Effect of alumina addition on the microstructure properties of plasma-sprayed zirconia-alumina coatings, Optoelectronics and Advanced Materials - Rapid Communications, 7, 7-8, July-August 2013, pp.585-589 (2013).

Submitted at: Oct. 6, 2012

Accepted at: July 11, 2013